Volume 8, Issue 1, January 2020, Page: 5-11
Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar
Qiang Sun, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Yuliang Gao, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Liyan Wang, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Received: Dec. 21, 2019;       Accepted: Jan. 8, 2020;       Published: Jan. 31, 2020
DOI: 10.11648/j.sjac.20200801.12      View  37      Downloads  27
Abstract
A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.
Keywords
Wood Vinegar, DLLME-SFO, GC/MS, Organic Components
To cite this article
Qiang Sun, Yuliang Gao, Liyan Wang, Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar, Science Journal of Analytical Chemistry. Vol. 8, No. 1, 2020, pp. 5-11. doi: 10.11648/j.sjac.20200801.12
Copyright
Copyright © 2020 Authors retain the copyright of this article.
This article is an open access article distributed under the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
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